Научная статья на тему 'Energy efficiency of the disinfection treatment of liquid foodstuffs by high-voltage pulse effects'

Energy efficiency of the disinfection treatment of liquid foodstuffs by high-voltage pulse effects Текст научной статьи по специальности «Электротехника, электронная техника, информационные технологии»

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Ключевые слова
generator of high-voltage pulses / transformer / capacitor / multi-gap discharger / multichannel switch / working chamber / disinfecting food treatment / генератор высоковольтных импульсов / трансформатор / конденсатор / многозазорный разрядник / многоканальный разрядник / рабочая камера / обеззараживающая обработка пищевых продуктов

Аннотация научной статьи по электротехнике, электронной технике, информационным технологиям, автор научной работы — M. I. Boyko, A. V. Makogon, A. I. Marynin

Purpose. Experimentally determine the rational modes and energy efficiency of decontamination treatment of flowing food products using high-voltage impulse actions in comparison with traditional pasteurization. Methodology. We used pulse generation method with the help of a step-up transformer, high-voltage pulse capacitors and spark gaps with a system of peaking of pulse front to obtain high-voltage pulses in working chambers the generator load. The pulses on the load were measured by a low-resistance resistive voltage divider, were transmitted over a broadband coaxial cable and recorded using an analog C8-12 oscilloscope or a Rigol DS1102E digital oscilloscope with a bandwidth of 100 MHz for each. The working chambers were filled with water, milk or milk whey and consisted of an annular hull made of PTFE and metal electrodes forming the bottom and the chamber cover having flat linings of food grade stainless steel for contact with the food product inside the chamber. Results. We obtained high-voltage pulses on the generator load with a base duration of 300 to 1200 ns at pulse repetition rates up to 500 pulses per second. We obtained experimentally the amplitude of the voltage pulses on the generator load up to 75 kV, and the electric field strength up to 35 kV/cm in working chambers with a gap of 22 mm and up to 50 kV/cm in working chambers with a gap of 15 mm. These characteristics of the pulses allowed complete and irreversible inactivation of microorganisms in food liquids in working chambers. Originality. We showed that there are modes of treatment food products with the help of highvoltage pulse actions, which allow better to preserve the biological and nutritional value of the products in comparison with heat treatment with their complete disinfection and at a significantly lower specific energy consumption. Practical value. The experimental regimes for treating milk, whey and water with reduced specific energy consumption open the prospect of industrial application of a complex of high-voltage pulse actions for the disinfecting treatment of water-containing food products. References 7, tables 3, figures 10.

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Цель. Экспериментально определить рациональные режимы и энергоэффективность обеззараживающей обработки текучих пищевых продуктов при помощи высоковольтных импульсных воздействий в сравнении с традиционной пастеризацией. Методика. Для получения высоковольтных импульсов на рабочих камерах – нагрузке генератора применена методика генерирования импульсов при помощи повышающего трансформатора, высоковольтных импульсных конденсаторов и разрядников с системой обострения фронта импульсов. Импульсы на нагрузке измерялись при помощи низкоомного резистивного делителя напряжения, передавались по широкополосному коаксиальному кабелю и регистрировались при помощи аналогового осциллографа С8-12 или цифрового осциллографа Rigol DS1102E с полосой пропускания 100 МГц у каждого. Рабочие камеры заполнялись водой, молоком или молочной сывороткой и состояли из кольцеобразного корпуса, выполненного из фторопласта, и металлических электродов, образующих дно и крышку камеры, имеющих плоские накладки из пищевой нержавеющей стали для контакта с пищевым продуктом внутри камеры. Результаты. Получены высоковольтные импульсы на нагрузке генератора с длительностью по основанию 300-1200 нс при частотах следования импульсов до 500 имп/с. Экспериментально полученные амплитуды импульсов напряжения на нагрузке генератора – до 75 кВ, а напряженности электрического поля – до 35 кВ/см в рабочих камерах с зазором 22 мм и до 50 кВ/см в рабочих камерах с зазором 15 мм. Указанные характеристики импульсов позволили осуществить полную и необратимую инактивацию микроорганизмов в пищевых жидкостях в рабочих камерах. Научная новизна. Показано, что существуют режимы обработки пищевых продуктов при помощи высоковольтных импульсных воздействий, позволяющие лучше сохранить биологическую и пищевую ценность продуктов по сравнению с тепловой обработкой при их полном обеззараживании и при существенно меньших удельных энергозатратах. Практическая значимость. Полученные экспериментально режимы обработки молока, молочной сыворотки и воды с уменьшенными удельными энергозатратами открывают перспективу промышленного применения комплекса высоковольтных импульсных воздействий для обеззараживающей обработки водосодержащих пищевых продуктов. Библ. 7, табл. 3, рис. 10.

Текст научной работы на тему «Energy efficiency of the disinfection treatment of liquid foodstuffs by high-voltage pulse effects»

UDC 621.373; 577.2; 577.3

doi: 10.20998/2074-272X.2018.3.07

M.I. Boyko, A.V. Makogon, A.I. Marynin

ENERGY EFFICIENCY OF THE DISINFECTION TREATMENT OF LIQUID FOODSTUFFS BY HIGH-VOLTAGE PULSE EFFECTS

Purpose. Experimentally determine the rational modes and energy efficiency of decontamination treatment of flowing food products using high-voltage impulse actions in comparison with traditional pasteurization. Methodology. We used pulse generation method with the help of a step-up transformer, high-voltage pulse capacitors and spark gaps with a system of peaking ofpulse front to obtain high-voltage pulses in working chambers - the generator load. The pulses on the load were measured by a low-resistance resistive voltage divider, were transmitted over a broadband coaxial cable and recorded using an analog C8-12 oscilloscope or a Rigol DS1102E digital oscilloscope with a bandwidth of 100 MHz for each. The working chambers were filled with water, milk or milk whey and consisted of an annular hull made of PTFE and metal electrodes forming the bottom and the chamber cover having flat linings of food grade stainless steel for contact with the food product inside the chamber. Results. We obtained high-voltage pulses on the generator load with a base duration of 300 to 1200 ns at pulse repetition rates up to 500 pulses per second. We obtained experimentally the amplitude of the voltage pulses on the generator load up to 75 kV, and the electric field strength up to 35 kV/cm in working chambers with a gap of 22 mm and up to 50 kV/cm in working chambers with a gap of 15 mm These characteristics of the pulses allowed complete and irreversible inactivation of microorganisms in food liquids in working chambers. Originality. We showed that there are modes of treatment food products with the help of highvoltage pulse actions, which allow better to preserve the biological and nutritional value of the products in comparison with heat treatment with their complete disinfection and at a significantly lower specific energy consumption. Practical value. The experimental regimes for treating milk, whey and water with reduced specific energy consumption open the prospect of industrial application of a complex of high-voltage pulse actions for the disinfecting treatment of water-containing food products. References 7, tables 3, figures 10.

Key words: generator of high-voltage pulses, transformer, capacitor, multi-gap discharger, multichannel switch, working chamber, disinfecting food treatment.

Цель. Экспериментально определить рациональные режимы и энергоэффективность обеззараживающей обработки текучих пищевых продуктов при помощи высоковольтных импульсных воздействий в сравнении с традиционной пастеризацией. Методика. Для получения высоковольтных импульсов на рабочих камерах -нагрузке генератора применена методика генерирования импульсов при помощи повышающего трансформатора, высоковольтных импульсных конденсаторов и разрядников с системой обострения фронта импульсов. Импульсы на нагрузке измерялись при помощи низкоомного резистивного делителя напряжения, передавались по широкополосному коаксиальному кабелю и регистрировались при помощи аналогового осциллографа С8-12 или цифрового осциллографа Rigol DS1102E с полосой пропускания 100 МГц у каждого. Рабочие камеры заполнялись водой, молоком или молочной сывороткой и состояли из кольцеобразного корпуса, выполненного из фторопласта, и металлических электродов, образующих дно и крышку камеры, имеющих плоские накладки из пищевой нержавеющей стали для контакта с пищевым продуктом внутри камеры. Результаты. Получены высоковольтные импульсы на нагрузке генератора с длительностью по основанию 300-1200 нс при частотах следования импульсов до 500 имп/с. Экспериментально полученные амплитуды импульсов напряжения на нагрузке генератора - до 75 кВ, а напряженности электрического поля - до 35 кВ/см в рабочих камерах с зазором 22 мм и до 50 кВ/см в рабочих камерах с зазором 15 мм. Указанные характеристики импульсов позволили осуществить полную и необратимую инактивацию микроорганизмов в пищевых жидкостях в рабочих камерах. Научная новизна. Показано, что существуют режимы обработки пищевых продуктов при помощи высоковольтных импульсных воздействий, позволяющие лучше сохранить биологическую и пищевую ценность продуктов по сравнению с тепловой обработкой при их полном обеззараживании и при существенно меньших удельных энергозатратах. Практическая значимость. Полученные экспериментально режимы обработки молока, молочной сыворотки и воды с уменьшенными удельными энергозатратами открывают перспективу промышленного применения комплекса высоковольтных импульсных воздействий для обеззараживающей обработки водосодержащих пищевых продуктов. Библ. 7, табл. 3, рис. 10.

Ключевые слова: генератор высоковольтных импульсов, трансформатор, конденсатор, многозазорный разрядник, многоканальный разрядник, рабочая камера, обеззараживающая обработка пищевых продуктов.

Introduction. Traditional thermal methods of disinfecting treatment (pasteurization and thermal sterilization) of liquid food products, wine materials, beverages are energy-consuming and do not allow to preserve their initial biological and nutritional value to a sufficient extent [1, 2]. One of the most promising ways of non-thermal disinfection treatment of products is the way of processing by means of a complex of high-voltage impulse actions (CHVIA). The English-language scientific literature uses the term PEF-treatment (PEF - pulsed electric field, treatment with a pulsed electric field). Most

liquid food products are water-containing. Therefore, the important question is also about rational modes of decontaminating water treatment by using CHVIA.

The goal of the work is to experimentally determine the rational modes and energy efficiency of decontaminating treatment of liquid food products by means of high-voltage impulse actions in comparison with traditional pasteurization.

Experimental installation. To carry out experimental studies, we used a facility, which was first

© M.I. Boyko, A.V. Makogon, A.I. Marynin

described in [3]. The electrical circuit of the installation with the control system is shown in Fig. 1.

Three-phase power supply

a

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the transformer Tr. By pressing the button SB2, the pump electric motor M is switched off.

Working chambers. The working chambers (WCH) which are the load for the CHVIA installation are divided into stationary and flowing. In stationary chambers, portions of the product are replaced manually, and in flow chambers through the flow through the chamber which provides the pump and a pumping system. The latter contains containers for feeding and receiving the treated liquid product and hoses. It is in the WCH that energy is released which is initially stored in the main high-voltage capacitor of the installation.

Typical stationary and flow chambers are shown in Fig. 2 and Fig. 3, respectively.

Fig. 1. Electrical circuit of the CHVIA installation with a control system

The installation consists of low-voltage and highvoltage parts. The high-voltage part consists of a generator of high-voltage pulses and a load - a working chamber WCH. The generator contains a start cascade (C1, DC1) and two cascades of sharpening (C2, DC2 and C3, DC3). Each cascade contains a capacitor and an discharger. The discharger DC1 of the start cascade is multi-gap. All arresters are multi-channel. In the simplest mode of operation, only the first cascade is used. The disadvantage of this mode is the insufficient steepness of the pulse front on the load - the WCH working chamber. Therefore, the main amount of the experiments was carried out using all three cascades.

After connecting to a three-phase power supply, during flow processing, pressing the button SB1 starts the pump electric motor M which pumps the processed product through the WCH working chamber. Pressing the button SB3 energizes the relay K2, its contacts K2.1, K2.2, K2.3 are closed, and the phase voltage of the power network through the filter L0 - CO is fed to the primary (low-voltage) winding of the transformer Tr starting the installation. As a result, on the load - the WCH working chamber, pulses are formed of high voltage (up to 120 kV) and current of both polarities with repetition frequency up to 500 pulses. The button SB4 switches off the supply of voltage to the filter L0 - CO and to the primary winding of

Fig. 2. Variant of stationary WCH with cover - electrode located near

output

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Fig. 3. a - variant of the design of the flowing technological WCH: 1, 2 - electrodes, 3 - internal volume of the chamber, 4 - dielectric housing; b - WCH

a

Experimental studies of CHVIA methods for the treatment (PEF-treatment) of food products and water treatment. We experimentally investigated the effect of CHVIA treatment on microbiological contamination, sanitary and hygienic properties and organoleptic parameters of milk, milk whey and water. The investigations were carried out in different treatment modes in stationary and flowing WCHs at the CHVIA installation described above.

A photo of an operating CHVIA installation during the experiments is shown in Fig. 4. The product to be processed was poured into a WCH which was previously sterilized with an alcohol burner, and the chamber was closed with a sterilized lid. Two types of cameras were used: with an interelectrode gap (the distance between the disk cover of the chamber and its bottom) of 15 mm and with an interelectrode gap of 22 mm. We varied the treatment time from 10 s to 30 s. Fig. 5 shows a WCH with an interelectrode gap of 22 mm.

Fig. 4. Photo of operating CHVIA installation

To measure the characteristics of pulses on the load of the CHVIA installation - the working chamber, a resistive low-resistance voltage divider with a division

coefficient ^d=1000 was used. As the recording device an analog storage oscilloscope C8-12 with a bandwidth of 100 MHz and a digital oscilloscope RIGOL DS1102E with a bandwidth of 100 MHz were used.

To protect against electromagnetic interference, the oscilloscope was located in a shielding cabin with a door screened circuit along the contour. The signal from the low-voltage arm of the voltage divider to the oscilloscope in the measuring cabinet was fed using a coaxial cable with a double braid. The door in the measuring cabinet can be opened and closed tightly both from the outside and from the inside.

d

Fig. 5. Working chamber with an interelectrode gap of 22 mm: a - body made of fluoroplastic, b - cover, c - interelectrode gap of 22 mm, d - cover near the chamber

The inactivating effect of CHVIA on various milk products (milk, whey, yogurt), as well as water, was investigated. To do this, our colleagues, co-executors from the National University of Food Technologies (NUFT), the city of Kiev, prepared water for experiments. They took water «Sofia Kiev» and infested it with bacteria of the E-coli group. At each treatment mode of all the fluids studied, three repetitions were performed.

The values of the interelectrode gap in the spark dischargers had the following values: for a multi-gap discharger (MGD), the value of an individual gap is approximately 5 mm, for the first sharpening discharger approximately 20 mm, for a second sharpening discharger approximately 20 mm. At the same time, the number of gaps involved in the MGD was from 4 to 7 inclusive.

The treatment of samples of liquid products and water in the WCH in all modes was carried out by pulses of both polarities. During the period of 20 ms of the AC network voltage during the half-period of the positive voltage of 10 ms, approximately 4 pulses of the same polarity were applied to the WCH, and about 4 pulses of a different polarity were applied to the WCH during the half-period of the negative voltage of 10 ms.

Results of experimental studies of the methods of CHVIA treatment (PEF-treatment). Fig. 6 shows an oscillogram of pulses on the WCH with milk at 7 ruptured gaps of 8 in a multi-gap discharger - MGD without the influence of electromagnetic interference and with a clearly visible pulse front.

Fig. 6. Typical oscillogram of the voltage pulse on the WCH with raw milk. The scale division along the time axis is

50 ns/div; along the axis of the process is 20 kV/div. In multi-gap discharger 7 gaps of 8 are ruptured.

The gap in the WCH is d = 22 mm

It follows from the oscillogram that the pulse front duration in milk is about 20 ns and the pulse duration along the base before passing through zero is about 300 ns. Amplitude of the voltage pulse is not less than 60 kV. From this it follows that the amplitude of the electric field strength in milk is 60/2.2-27.3 kV/cm. It is also important that in milk which has a resistivity less than tap water or table water, the pulse shape is slightly oscillatory.

Fig. 7 shows a typical oscillogram of the pulse voltage on the WCH with water, contaminated with E-coli. The oscillogram was obtained using a digital oscilloscope Rigol 1102 E.

From the oscillogram in Fig. 7 it follows that the amplitude of the voltage on the WCH with water in this mode is not less than 72 kV, the pulse duration on the base

is approximately 1200 ns, and the pulse shape is aperiodic, unipolar, does not pass through the zero line. The zero line is shown in Fig. 7 and further by the arrow located to the left of the oscillogram.

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Fig. 7. Typical oscillogram of the voltage pulse on a working chamber with water «Sofia Kiev» seeded by E-coli. The scale division along the time axis is 200 ns/div; along the axis of the process is 20 kV/div. In the multi-gap discharger 6 gaps of 8 are ruptured. The gap in the WCH is d=22 mm. A low-resistance resistive voltage divider with division coefficient kd =2000 is used

Two additional bursts at the fall of the pulse on this oscillogram, as well as on other oscillograms, are due to the presence of three high-voltage capacitive storage devices: the main one and two sharpening ones. The front part of the pulse is due to the last (second) sharpening cascade with the second sharpening capacitive storage, the first additional burst at the pulse decay is due to the presence of the first cascade of sharpening with the first sharpening capacitive storage, and the second additional surge at the pulse decay is due to the presence of the main high-voltage capacitive storage device.

The results of microbiological analyzes of water are given in Table 1.

Table 1

Detection of the bacteria of the family E.coli in water

The name of the indicator (units of measure CFU/cm3) Results of investigations, CFU/cm3 Approximated treatment mode, (E, kV/cm) Calculated treatment mode, (E, kV/cm) Treatment duration (t, s)

Water sterile. Dilution E.coli 106 210 30 20.09 10

Water sterile. Dilution E.coli 106 0 30 31.8 20

Water sterile. Dilution E.coli 108 60 30 19.0 10

Water sterile. Dilution E.coli 108 0 30 1.8 20

*Note: CFU - colony forming units.

the WCH with milk whey.

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Fig. 8. Typical oscillogram of the voltage pulse on a working chamber with milk whey. The scale division along the time axis is 200 ns/div; along the axis of the process is 10 kV/div. In the multi-gap discharger 6 gaps of 8 are ruptured. The gap in the WCH is d=22 mm. A low-resistance resistive voltage divider with division coefficient kd =1000 is used

The pulse duration along the base on the oscillogram (Fig. 8) is approximately 350 ns. The pulse shape is oscillatory with a large decrement of oscillations. The amplitude of the voltage pulse on this oscillogram is approximately 45 kV, and the amplitude of the voltage is approximately 20.45 kV/cm.

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In Fig. 9 shows a typical oscillogram of the pulse voltage on the WCH with raw milk.

The results of microbiological analyzes of milk whey treated with CHVIA pulses, a sample oscillogram of which is presented in Fig. 8, are given in Table 2-5.

[»¡IB 10.0UIS Time 203.0ns O+0.0000s

Fig. 9. Typical oscillogram of the voltage pulse on a working chamber with raw milk. The scale division along the time axis is 200ns/div; along the axis of the process is 10 kV/div. In the multi-gap discharger 6 gaps of 8 are ruptured. The gap in the WCH is d=22 mm. A low-resistance resistive voltage divider with division coefficient kj^ 1000 is used

Table 2

The results of the analyzes on the detection of E.coli family bacteria in milk whey after CHVIA treatment

The name of the indicator, units of measure CFU/cm3 E.coli Result, CFU/cm3

at E=30 kV/cm, total treatment duration t=10 s and dilution 106 30

at E=30 kV/cm, total treatment duration t=20 s and dilution 106 0

at E=30 kV/cm, total treatment duration t=10 s and dilution 108 20

at E=30 kV/cm, total treatment duration t=20 s and dilution 108 0

Table 3

Physicochemical parameters of initially raw milk after CHVIA treatment

The name of the indicator, units of measure ND for testing techniques Investigation result Indicator value in accordance with ND Compliance with ND

1 2 3 4 5

Determination of the mass portion of vitamin C by titrimetric method in food products

mass part of vitamin C, ppm GOST 30627.2-98 5.0 not regulated corresponds to ND

Determination of peroxidase by the method of qualitative analysis in food products

peroxidase for baked, ultra-pasteurized, sterilized milk DSTU 7380:2013 detected absent does not correspond

Determination of phosphatase of milk and milk products by method of qualitative analysis

phosphatase for pasteurized milk DSTU 7380:2013 not detected absent corresponds

From Table 2 it follows that after complete treatment of milk whey in the WCH during 20 s by high-voltage pulses (see Fig. 8) complete inactivation of E.coli bacteria is guaranteed. When treated during 10 s from 20 to 30 colony forming units remain not inactivated. Thus, the existence of a mode of complete guaranteed inactivation at CHVIA treatment of products was confirmed experimentally. In control (not treated by CHVIA) samples of milk whey, a continuous growth of E.coli bacteria (>>1000 CFU/cm3) was observed.

The pulse duration along the base on the oscillogram in Fig. 9 is approximately 350 ns. The pulse shape is oscillatory with a large decrement of oscillations (weakly vibrational). The amplitude of the voltage pulse on this oscillogram is approximately 60 kV, and the amplitude of the electric field strength is approximately 60/2.2=27.3 kV/cm.

The results of laboratory studies of the physicochemical parameters of milk after CHVIA treatment (see Fig. 9) are given in Table 3.

From the results given in Table 6 it follows that in CHVIA treated milk there is a peroxidase enzyme, the absence of which is characteristic of baked, ultra-pasteurized, sterilized milk, that is, milk that was amenable to processing at high temperatures (greater than 100 °C). However, in CHVIA treated milk, no enzyme phosphatase was detected, the absence of which is characteristic of pasteurized milk. In addition, from the data of Table 6 it follows that the amount of vitamin C which is very sensitive to different treatments, after CHVIA treatment has remained at the level meeting the requirements of normative documentation (ND), that is, CHVIA treatment is soft processing. All analyzes (microbiological and sanitary-hygienic) of treated and control samples of water-containing foods and water were conducted by specialists of the public utility «Sanepidservice» (public unity «SES», the Kharkiv city). This enterprise is accredited by the National Agency of Ukraine for Accreditation (Accreditation Certificate No. 2H1207 of 25.02.2015).

Energy efficiency of high-voltage prototype of CHVIA installation. Energy efficiency is determined by two components: high degree of microbiological (microbial) disinfection of the processed product at a given specific energy input and reduced specific energy consumption in comparison with known methods (for example, thermal sterilization and pasteurization). The first component can be estimated by conducting CHVIA processing and making the corresponding microbiological analyzes of the processed product (water, milk, milk whey). The second component of energy efficiency can be estimated on the basis of what part of the energy consumed from the power supply network by the CHVIA installation was delivered to the WCH and there it was dissipated leading to the required degree of inactivation of microorganisms in the water. Since in all elements of the CHVIA installation, including in high-voltage capacitors, a transformer and dischargers, not more than 0.1 total energy consumed from the network dissipates in total, efficiency of the installation can be estimated as 0.9, or 90% [4-6]. It is more difficult to estimate how much energy is dissipated in the WCH. We do this with the help of oscillograms of voltage pulses on the WCH with the treated product. A typical oscillogram of the voltage pulse on a chamber with water being treated is shown in Fig. 10.

RIGOL STOP О w^m^Jmmmmm f О 0.00uU

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Fig. 10. Typical voltage pulse oscillogram on a working chamber with treated water

The three peaks (maximums), as mentioned above, on the oscillogram correspond to the processes of discharge of three capacitors (C1, C2, C3) on the load -the working chamber, in this case filled with water (see Fig. 1). The first (largest) peak after the pulse front is the maximum voltage on the WCH due to the energy input to the chamber from the most low-inductive discharge circuit with the capacitive storage C3. The second peak corresponds to the process of connecting and discharging capacitor C2 on the WCH. The third peak corresponds to the process of connecting to the discharge on the WCH of capacitance C1, more remote from the WCH and having the greatest inductance.

Energy which is released in the WCH during processing can be estimated by the formula

E = nT | iudt = nTiavuavt, (1)

where i is the current as a temporal function, u is the voltage as a temporal function, iav is the averaged current, uav is the averaged voltage, t is the duration of one pulse at half-height - the length of time during which the energy of the pulse is released in the WCH, n is the pulse repetition rate, T is the treatment duration.

We suppose that water in the WCH is a purely resistive load. The pulse duration is determined from the oscillograms.

According to the voltage oscillogram, it is possible to find the active resistance Rwch of water in the chamber, knowing the value of the high-voltage capacitance Chv in which energy is accumulated before after transformation in the transformer HOM 100/100 [7]

(t/0.7) = Rwch-Chv, (2)

where t is the pulse duration at half-height, and t/0.7 is the pulse duration before the measured value decreases from the amplitude value in e ~ 2.71828 time.

For our installation Chv ~ 10-8 F, t ~ 380 ns (see oscillogram in Fig. 10). Thus

Rwch = (t/0.7)/Chv = (3.8-10-7/0.7)/10-8 ~ 54.3 Q.

Taking into account that uav ~ 40 kV, iav = uJRwch = = 40000 V/54.3 Q ~ 736.65 A. From here it follows that at n = 400 pulses/s, T = 10 s, t = 3.8-10-7 s, the energy Ewch dissipated in the chamber is Ewch=nTiavuavt = 400 pulses/s x X 10 s x 736.65 A X40000 V x 3.8 x 10-7 s = 16 x 736.65 x x 3.8 ~ 44.8 kJ.

Here, the averaged power P consumed in the WCH with water approximately equals P = Ewch/T = 44.8 kJ/10 s ~ ~ 4.5 kW.

The energy E1C1 initially stored in the high-voltage discharge circuit in the capacitor C1 before each discharge can be estimated by the formula

E1C1 = C1-uC12/2 ~ 10-8-(50-103)2/2 = 12.5 J.

We estimate the total energy ECT accumulated in C1 during time T

Ec1 = nTEia = 400 pulses/s x 10 s x 12.5 J = = 50000 J = 50 kJ. E/EC1 ~ 44.8/50 = 0.896.

The resistivity of the water in WCH can be estimated by the formula

p = RwchxS/1, (3)

where S is the cross-sectional area of WCH with the liquid to be treated relative to the current flow direction, l is the length of the interelectrode gap in the WCH i.e. its (working chamber's) height.

At S = 3.14-4.752-10-4 = 7.1-10-3 m2, l = 1.510-2 m: p = 54.3 Q x 7.1 x 10-3 m2/1.5-10-2 m = 25.7 Q-m.

We estimate the heating At of water in a non-current (stationary) WCH for T = 10 s with energy E ~ 44.8 kJ dissipated in the chamber. If we assume that half of this energy was used to heating the water, and the other half to heating the metal electrodes - the covers of the WCH and its insulating (fluoroplastic) housing, then

E = 2-c-V-y-At, i.e. At = 0.5-E/(c-V-y), (4) where c = 4200 J/(kg-K) is the specific heat of water, V is the water volume in the WCH, y = 103 kg/m3 is the density of water.

V = S-l = 7.1-10-3 m2-1.5-10-2 m = 10-4 m3.

So:

At = 0.5 -44.8- 103J/(4200 J/(kg-K)> >10-4 m3-103 kg/m3) = 53.3 K.

The obtained calculated result is in good agreement with the experimental result on heating water in a given WCH under CHVIA treatment. The measurements were carried out with a M890G tester using a thermocouple. The measured temperature drop from the initial (start) tstart to the final tfi„ai was AiOT = i« - tstart = 74 - 20 = 54 K. Hence the conclusion follows that practically all the electromagnetic energy reaching the WCH is released in it in the form of heat. This is of fundamental importance, since both electromagnetic factors (electric and magnetic field strength, voltage and current in the WCH) and thermal energy are synergistically directed (unidirectional) factors. This unidirectional effect leads to an increase in the degree of inactivation of microorganisms in the flowable liquid products processed in the WCH. At the same time, all energy supplied to the WCH is used for its intended purpose - microbiological disinfection of the product processed in the chamber. If we now assume that all the heat released in the chamber is transferred through a heat exchanger to an unprocessed product that has not yet passed through the WCH, then the efficiency ne for the given technological process ne = 85-99.5%.

An important indicator is also the specific energy consumption of Esp, that is, the amount of energy expended for processing a unit (for example, units of volume or mass) of the product. At CHVIA processing in industrial flowing option, when rational heat exchange is involved, this is the amount of electromagnetic energy Eflow introduced into the WCH which in the chamber passes into thermal energy. Here, the product heating Atflow is guaranteed in the flow mode, while it flows through the WCH, by several K (for example, by 5 K) and the transition from the subcritical temperature to the supercritical temperature of the product which ensures irreversible inactivation of microorganisms under the action of high external pulsed electric field.

Estimation of Eflow and Esp

Efiow = c-V-y-Atflow = 4200 J/(kg-K)x10-4 m3x103 kg/m3x x5 K = 2100 J;

Esp = EflJV = c-y-Atflow = 2100 J/10-4 m3 = 2.1-107 J/m3 = = 2.1-104 kJ/m3 = (21000/3600) kW-h/m3 = = 5.83 kW-h/m3.

Thus, the estimated value of the specific energy consumption in the flowing mode at CHVIA treatment of products is Esp = 5.83 kWh/m3. AT the traditional scheme of microbiological milk disinfection (with the help of heat treatment - pasteurization), the specific energy consumption is more, at least 4 times [1, 2].

Conclusions.

1. Rational modes of operation of CHVIA installation for the tested working chambers take place at amplitudes of pulsed electric field strength E = 30 kV/cm in the liquid in the working chamber and at the treatment duration of 20 s with high-voltage pulses of duration 300-1200 ns at pulse repetition rate n = 400 pulses/s.

2. At rational modes in the treated water, milk whey and milk, the demonstrative E.coli bacteria are completely and irreversibly inactivated. In this case, the enzyme peroxidase in milk is preserved. Consequently, the tested rational mode of disinfecting milk treatment is milder than the mode of thermal sterilization, and approximately corresponds to pasteurization.

3. The amount of vitamin C, highly sensitive to various treatments, after treating milk in rational modes is maintained at a level that meets the requirements of regulatory documentation, that is, CHVIA treatment is a soft treatment that preserves the biological and nutritional value of the products.

4. Estimated value of specific energy consumption in flowing mode AT CHVIA treatment of products is Esp = 6 kWh/m3, which is about 4 times less than at traditional heat treatment. At the same time, the energy efficiency of the proposed complex of high-voltage pulse actions is 4 times higher compared with pasteurization.

5. The results of the performed investigations open the prospect of the industrial application of a complex of highvoltage pulse actions for the disinfecting treatment of water-containing food products.

REFERENCES

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Received 13.03.2018

M.I. Boyko1, Doctor of Technical Sciences, Professor, A.V. Makogon1,

A.I. Marynin2, Candidate of Technical Sciences, Associate Professor,

1 National Technical University «Kharkiv Polytechnic Institute», 2, Kyrpychova Str., Kharkiv, 61002, Ukraine,

phone +380 57 7076245, e-mail: [email protected]

2 National University of Food Technologies, 68, Volodymyrska Str., Kyiv, 01601, Ukraine, e-mail: [email protected]

How to cite this article:

Boyko M.I., Makogon A.V., Marynin A.I. Energy efficiency of the disinfection treatment of liquid foodstuffs by highvoltage pulse effects. Electrical engineering & electromechanics, 2018, no.3, pp. 53-60. doi: 10.20998/2074-272X.2018.3.07.

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